Glyoxal → HCID 15099950, 화합물

HRID 1651502노트

반응식

HRID 1651502 반응식
[CH2:1]([PH2:4])[CH2:2][CH3:3].[CH:5]([CH:7]=[O:8])=[O:6]>O1CCCC1>[CH2:1]([P:4]1[CH:5]([OH:6])[CH:7]([OH:8])[P:4]([CH2:1][CH2:2][CH3:3])[CH:5]([OH:6])[CH:7]1[OH:8])[CH2:2][CH3:3]

참가 물질

4

반응물 2

HCID 7860GlyoxalHCID 14647240Propylphosphane

생성물 1

HCID 15099950HCID 15099950, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

Following the procedure of Example 1, mono-n-propylphosphine, in tetrahydrofuran, as solvent, is reacted with a 40% aqueous glyoxal solution, to give 1,4-di-n-propyl-2,3,5,6-tetrahydroxy-1,4-diphosphorinane, a solid melting at 131-133° C.

출처 및 근거

ORD 기록
ord-727e99fbc7df464cabd984d6b14d54a7
출처 데이터셋
uspto-grants-1990_05
특허 번호
US04929393

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