Cyclopentene → Dichlorodicyclopentylsilane

HRID 1653858노트

반응식

HRID 1653858 반응식
[CH:1]1[CH2:5][CH2:4][CH2:3][CH:2]=1.[Cl:6][SiH2:7][Cl:8]>>[CH:1]1([Si:7]([CH:1]2[CH2:5][CH2:4][CH2:3][CH2:2]2)([Cl:8])[Cl:6])[CH2:5][CH2:4][CH2:3][CH2:2]1

참가 물질

3

반응물 2

HCID 8882CyclopenteneHCID 61330Dichlorosilane

생성물 1

HCID 10857476Dichlorodicyclopentylsilane

실험 절차

Cyclopentene in an amount of 136 g (2.00 moles) was made to react with dichlorosilane under various conditions set forth in Table 1, and then the solvent was distilled away. Thus, in analogy with Example 1, dicyclopentyldichlorosilane having a boiling point of 104° C./5 mmHg was obtained in various yields. The yield attained under each reaction condition is shown in Table 1.

후처리

  1. distillationthe solvent was distilled away

출처 및 근거

ORD 기록
ord-70339c750cdd4f40bfd6a2d3452b066b
출처 데이터셋
uspto-grants-1995_04
특허 번호
US05403947

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