Hydrochloric Acid → 26431-60-7

반응식

Br[CH2:2][C:3]1[O:4][CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.C1N2CN3CN(C2)CN1C3.Cl.[OH2:23]>>[F:9][C:8]([F:11])([F:10])[C:6]1[CH:7]=[C:3]([CH:2]=[O:23])[O:4][CH:5]=1

참가 물질

반응물 4

HCID 313Hydrochloric Acid

HCID 962Water2회

HCID 4101Hexamethylenetetramine

HCID 218197532-(Bromomethyl)-4-(trifluoromethyl)furan

생성물 1

HCID 2181974626431-60-7

실험 절차

2.95 g of the product of Stage E, 9 ml of water and 3.6 g of hexamethylenetetramine were refluxed for 1 hour. 9 ml of concentrated hydrochloric acid were added. Reflux was maintained for an additional 1 hour and the mixture was allowed to return to room temperature, diluted with water and extracted with methylene chloride. The extract was washed with water and dried and the solvent was evaporated to obtain 1.9 g of the expected product.