Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenethylamine → alpha-[(Phenethylcarbamoyl)methyl]cinnamic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenethylamine | HCID 1001 | — |
| 반응물 | Phenylitaconic anhydride | HCID 222996 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | alpha-[(Phenethylcarbamoyl)methyl]cinnamic acid | HCID 54394250 | 70% |
반응 단계
226 mg (1.2 mmol) of benzalsuccinic acid anhydride were treated in 20 ml of methylene chloride with 0.15 ml of 2-phenethylamine and subsequently stirred at room temperature for 2 hours. The solvent was removed under reduced pressure and the residue was chromatographed on silica gel, to obtain 260 mg (70%) of α-[(phenethylcarbamoyl)methyl]cinnamic acid, MS: 309 (M)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05250517 |
| 출처 데이터셋 | uspto-grants-1993_10 |
| ORD ID | ord-c9ce86940efa48f98dcf91f9845cffae |
| 출처 메모 | uspto-grants-1993_10 |