Hydrochloric Acid → HCID 178479262, 화합물

HRID 1656054노트

반응식

HRID 1656054 반응식
[ClH:1].[NH2:2][C@@H:3]1[CH2:8][CH2:7][C@H:6]([C:9]([O:11]C)=[O:10])[CH2:5][CH2:4]1.Cl>O>[ClH:1].[NH2:2][C@@H:3]1[CH2:8][CH2:7][C@H:6]([C:9]([OH:11])=[O:10])[CH2:5][CH2:4]1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 178501209HCID 178501209, 화합물

생성물 1

HCID 178479262HCID 178479262, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Dissolve cis-4-amino-cyclohexanecarboxylic acid, methyl ester hydrochloride (1.5 g) in water (5 mL) and add concentrated hydrochloric acid (5 mL). Reflux under an argon atmosphere for 12 hours and evaporate the solvent in vacuo to give cis-4-amino-cyclohexanecarboxylic acid hydrochloride.

후처리

  1. temperatureReflux under an argon atmosphere for 12 hours
  2. customevaporate the solvent in vacuo

출처 및 근거

ORD 기록
ord-9c65247a21114259ac413ed1ae1ead2e
출처 데이터셋
uspto-grants-1993_10
특허 번호
US05252601

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