Dibutyltin oxide → Dibutyltin bis-ricinoleate

HRID 1657130

반응식

HRID 1657130 반응식
[CH2:1]([Sn:5](=O)[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].[C:11]([OH:31])(=[O:30])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]/[CH:19]=[CH:20]\[CH2:21][C@@H:22]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[OH:23]>C1(C)C=CC=CC=1>[C:11]([O-:31])(=[O:30])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]/[CH:19]=[CH:20]\[CH2:21][C@@H:22]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[OH:23].[C:11]([O-:31])(=[O:30])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]/[CH:19]=[CH:20]\[CH2:21][C@@H:22]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29])[OH:23].[CH2:1]([Sn+2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4]

참가 물질

4

반응물 2

HCID 61221Dibutyltin oxideHCID 643684Ricinoleic Acid

생성물 1

HCID 86747340Dibutyltin bis-ricinoleate

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

A mixture of dibutyltin oxide, 31.2 g (0.125 mole), ricinoleic acid, 74.25 g (0.25 mole), and 250 ml toluene were mixed and reacted as described in Example 1. Removal of toluene yielded 120 g (944 yield) of dibutyltin bis-ricinoleate, a yellow viscous liquid.

후처리

  1. additionwere mixed
  2. customreacted
  3. customRemoval of toluene

출처 및 근거

ORD 기록
ord-d98e29febf974c5b8e5f8a26b881742a
출처 데이터셋
uspto-grants-1993_10
특허 번호
US05256704

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