Hydrochloric Acid → HCID 12575251, 화합물

HRID 1657941노트

반응식

HRID 1657941 반응식
S(Cl)(Cl)=O.[C:5]([OH:15])(=O)/[CH:6]=[CH:7]/[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].[ClH:16]>>[C:5]([Cl:16])(=[O:15])/[CH:6]=[CH:7]/[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 24386Thionyl ChlorideHCID 5312586(E)-2-Nonenoic Acid

생성물 1

HCID 12575251HCID 12575251, 화합물수율 91%

반응 조건

온도
130 °C

실험 절차

Thionyl chloride (131 g, 1.1 mole) is added to trans-2-nonenoic acid (156 g, 1.0 mole). Reaction occurs immediately with the evolution of HCl and SO2. After the initial reaction subsides, the mixture is heated slowly to 130°C. The dark mixture is vacuum distilled to yield trans-2-nonenoyl chloride, b.p. 90°C/2 mm, 155 g, 91% yield.

후처리

  1. customReaction
  2. customAfter the initial reaction subsides
  3. distillationdistilled

출처 및 근거

ORD 기록
ord-571b4d0b56cf47a3b7999232a4246a05
출처 데이터셋
uspto-grants-1976_06
특허 번호
US03962321

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