Bromine → HCID 21529338, 화합물

HRID 1658385노트

반응식

HRID 1658385 반응식
[C:1]([C:4]1[CH:5]=[C:6]([CH:10]([CH3:16])[C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:7]=[CH:8][CH:9]=1)(=[O:3])[CH3:2].[Cl-].[Al+3].[Cl-].[Cl-].[Br:21]Br>CCOCC>[Br:21][CH2:2][C:1]([C:4]1[CH:5]=[C:6]([CH:10]([CH3:16])[C:11]([O:13][CH2:14][CH3:15])=[O:12])[CH:7]=[CH:8][CH:9]=1)=[O:3]

참가 물질

5

반응물 3

HCID 24408BromineHCID 6451240Aluminum(III) ChlorideHCID 12356932HCID 12356932, 화합물

생성물 1

HCID 21529338HCID 21529338, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

To a cooled vigorously stirred mixture containing ethyl 2-(m-acetyl phenyl)propionate (0.1 mole) dissolved in dry ether (100 ml) and a pinchful of aluminum chloride is added dropwise 0.1 mole bromine.

후처리

  1. temperatureTo a cooled vigorously stirred mixture

출처 및 근거

ORD 기록
ord-0b38972e4a144aa2ab82083bd55fc310
출처 데이터셋
uspto-grants-1976_06
특허 번호
US03963758

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