Hydrochloric Acid → HCID 86733570, 화합물

HRID 1658515노트

반응식

HRID 1658515 반응식
[CH3:1][N:2]1[CH2:8][C:7]([CH3:12])([N+:9]([O-:11])=[O:10])[CH2:6][N:5]2[CH2:13][CH2:14][CH2:15][CH2:16][CH:4]2[CH2:3]1.[ClH:17]>C(OCC)(=O)C>[ClH:17].[ClH:17].[CH3:1][N:2]1[CH2:8][C:7]([CH3:12])([N+:9]([O-:11])=[O:10])[CH2:6][N:5]2[CH2:13][CH2:14][CH2:15][CH2:16][CH:4]2[CH2:3]1

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 123395092,4-Dimethyl-4-nitrodecahydropyrido[1,2-a][1,4]diazepine

생성물 1

HCID 86733570HCID 86733570, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

Under agitation, a solution of 2.27 g. of 2,4-dimethyl-4-nitroperhydropyrido[1,2-a] [1,4] diazepine in 10 ml. of ethyl acetate is added to 20 ml. of 2N ethereal hydrochloric acid. The residue remaining after concentration is crystallized from chloroform; m.p. 189° C.

후처리

  1. concentrationafter concentration
  2. customis crystallized from chloroform

출처 및 근거

ORD 기록
ord-b2b1d4974385403ea4406162fc457004
출처 데이터셋
uspto-grants-1976_06
특허 번호
US03965103

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