1,3-Dinitrobenzene → Benzene, 1,3-dichloro-5-nitro-

HRID 1659983

반응식

[Cl:1]Cl.[Cl:3][C:4]1[CH:5]=[C:6]([N+]([O-])=O)[CH:7]=[C:8]([N+:10]([O-:12])=[O:11])[CH:9]=1.[N+](C1C=CC=C([N+]([O-])=O)C=1)([O-])=O>>[Cl:1][C:6]1[CH:7]=[C:8]([N+:10]([O-:12])=[O:11])[CH:9]=[C:4]([Cl:3])[CH:5]=1

참가 물질

반응물 3

HCID 74521,3-Dinitrobenzene

HCID 24526Chlorine

HCID 330981-Chloro-3,5-dinitrobenzene

생성물 1

HCID 12064Benzene, 1,3-dichloro-5-nitro-

실험 절차

A process as claimed in claim 4, which further comprises continuously introducing chlorine with a mixture of 5-chloro-1,3-dinitrobenzene and m-dinitrobenzene to the reaction at a constant rate and distilling of 1,3,5-trichlorobenzene and m-dichlorobenzene.

후처리

customto the reaction at a constant rate
distillationdistilling of 1,3,5-trichlorobenzene and m-dichlorobenzene

출처 및 근거

ORD 기록: ord-5991f122b38a4b5dbe15da6e21ff1b73
출처 데이터셋: uspto-grants-1981_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04306103

연결된 노트

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