Sulfur trioxide → 2-(4-Methylphenyl)-2-sulphoacetyl chloride
반응식
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]([Cl:11])=[O:10])=[CH:4][CH:3]=1.[S:12](=[O:15])(=[O:14])=[O:13]>ClCCl>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([CH:8]([S:12]([OH:15])(=[O:14])=[O:13])[C:9]([Cl:11])=[O:10])=[CH:6][CH:7]=1참가 물질
4
실험 절차
A solution of 4-methylphenylacetyl chloride (1.69 g, 10 mmole) in dichloromethane (20 ml) was treated with a suspension of sulphur trioxide--dioxane complex (15 mmole) in dichloromethane. The mixture was stirred at room temperature for eighteen hours and evaporated.
후처리
- customevaporated
출처 및 근거
- ORD 기록
- ord-35d560aac5b84defb7eaee8375b6e182
- 출처 데이터셋
- uspto-grants-1981_12
- 특허 번호
- US04308259
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