Nitric Acid → 3-Bromo-4-hydroxy-5-nitrobenzaldehyde

HRID 1663361

반응식

HRID 1663361 반응식
[Br:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[OH:10])[CH:5]=[O:6].[N+:11]([O-])([OH:13])=[O:12]>C(O)(=O)C>[Br:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[C:9]=1[OH:10])[CH:5]=[O:6]

참가 물질

4

반응물 2

HCID 944Nitric AcidHCID 763083-Bromo-4-hydroxybenzaldehyde

생성물 1

HCID 14943783-Bromo-4-hydroxy-5-nitrobenzaldehyde

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

3-Bromo-4-hydroxybenzaldehyde (250 mg) was dissolved in 5 ml of acetic acid. Nitric acid (52 μl) was added and the mixture was stirred for 3 h during which a solid formed. The solid was filtered off, washed with water and dried in vacuo.

후처리

  1. customformed
  2. filtrationThe solid was filtered off
  3. washwashed with water
  4. customdried in vacuo

출처 및 근거

ORD 기록
ord-1f5b60dd7fee4c75b87a95ec00faca54
출처 데이터셋
uspto-grants-2011_10
특허 번호
US08034945B2

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