Hydrochloric Acid → HCID 12824993, 화합물

HRID 1679508노트

반응식

HRID 1679508 반응식
[Cl:1][CH:2]([CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][C:15]([CH3:23])([CH3:22])[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:9][CH:8]=1)[C:3]([O-:5])=[O:4].[Na+].Cl>O>[Cl:1][CH:2]([CH2:6][C:7]1[CH:12]=[CH:11][C:10]([O:13][CH2:14][C:15]([CH3:23])([CH3:22])[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)=[CH:9][CH:8]=1)[C:3]([OH:5])=[O:4]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 23695280HCID 23695280, 화합물

생성물 1

HCID 12824993HCID 12824993, 화합물수율 91.4%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

In 5 ml of water is dissolved 350 mg of sodium 2-chloro-3-[4-(2,2-dimethyl-2-phenylethyloxy)phenyl]propionate, followed by the addition of 2-N hydrochloric acid. The oily substance separated out is extracted with ether. The extract is washed with water and the solvent is distilled off. The described procedure gives 300 mg of 2-chloro-3-[4-(2,2-dimethyl-2-phenylethyloxy)phenyl]propionic acid, as a yellow oily substance.

후처리

  1. customThe oily substance separated out
  2. extractionis extracted with ether
  3. washThe extract is washed with water
  4. distillationthe solvent is distilled off

출처 및 근거

ORD 기록
ord-bc91a5d96a9d417b8328ab8e47035566
출처 데이터셋
uspto-grants-1978_03
특허 번호
US04080505

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