Dibutylamine → HCID 23454947, 화합물

반응식

C(NCCCC)CCC.C(NNC1C=CC(N=C=S)=CC=1)=O.[CH:23]([NH:25][NH:26][C:27]1[CH:32]=[CH:31][C:30]([NH:33][C:34]([N:36]([CH2:44][C:45]2C=CC=[CH:47][CH:46]=2)[CH2:37][C:38]2C=CC=[CH:40][CH:39]=2)=[S:35])=[CH:29][CH:28]=1)=[O:24]>>[CH:23]([NH:25][NH:26][C:27]1[CH:28]=[CH:29][C:30]([NH:33][C:34]([N:36]([CH2:44][CH2:45][CH2:46][CH3:47])[CH2:37][CH2:38][CH2:39][CH3:40])=[S:35])=[CH:31][CH:32]=1)=[O:24]

참가 물질

반응물 3

HCID 8148Dibutylamine

HCID 20283022N'-(4-Isothiocyanatophenyl)formohydrazide

HCID 23454956HCID 23454956, 화합물

생성물 1

HCID 23454947HCID 23454947, 화합물

실험 절차

Di-n-butylamine (0.13 g, 0.001 mole) and 4-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.10 g (31 percent), m.p. 139°-141° C.

출처 및 근거

ORD 기록: ord-d0e69342806549b487cbcafa57ff9d45
출처 데이터셋: uspto-grants-1981_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04276364

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