Pyrrolidine → HCID 23454971, 화합물

반응식

N1CCCC1.C(NNC1(N=C=S)C=CC=CC1)=O.[CH:19]([NH:21][NH:22][C:23]1[CH:28]=[CH:27][C:26]([NH:29][C:30]([N:32]([CH2:40][C:41]2[CH:46]=[CH:45]C=CC=2)CC2C=CC=CC=2)=[S:31])=[CH:25][CH:24]=1)=[O:20]>>[CH:19]([NH:21][NH:22][C:23]1[CH:24]=[CH:25][C:26]([NH:29][C:30]([N:32]2[CH2:40][CH2:41][CH2:46][CH2:45]2)=[S:31])=[CH:27][CH:28]=1)=[O:20]

참가 물질

반응물 3

HCID 31268Pyrrolidine

HCID 23454956HCID 23454956, 화합물

HCID 23454969HCID 23454969, 화합물

생성물 1

HCID 23454971HCID 23454971, 화합물

실험 절차

Pyrrolidine (0.071 g, 0.001 mole) and 1-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.15 g (58 percent), m.p. 199°-201° C.

출처 및 근거

ORD 기록: ord-9efc38b06dfd4dd18f52ba090da51e72
출처 데이터셋: uspto-grants-1981_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04276364

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