참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,3-Diiodopropane | HCID 12314 | — |
| 반응물 | 3-Methyl-6-methylthiopurine | HCID 248868 | — |
| 생성물 | HCID 178503588 | HCID 178503588 | 28% |
반응 단계
A pressure tube, equipped with a magnetic stirring bar, was charged with Compound 2 (0.54 g, 3 mmole) and 1,3-diiodopropane (2.66 g, 9 mmole). The mixture was heated to ˜120° C. for 3 hours. The residue was extensively washed with ethyl acetate and diethyl ether and dried under vacuum to give 0.4 g of yellow solid Compound 3 (yield ˜28%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07737281B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-462658577d844d109c373b1b32a7fd9e |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
