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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1695233생성일: 2026년 10월 25일

Methanol → Methyl 4-(1-methylethoxy)benzoate

https://huagongshe.com/reaction/1695233

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물Sulfuric AcidHCID 1118—
반응물4-Isopropoxybenzoic acidHCID 72972—
생성물Methyl 4-(1-methylethoxy)benzoateHCID 301580767%

반응 단계

3.0 g of 4-isopropoxy-benzoic acid (16.7 mmol, 1.0 eq) were dissolved in MeOH (20 mL) and a catalytic quantity of sulfuric acid was added; the mixture was heated at reflux for 2 days. The solvent was then evaporated and the residue was dissolved in DCM and washed with 10% NaOH. The organic phases were dried and evaporated to give 2.2 g of title product (yield 67%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08163729B2
출처 데이터셋uspto-grants-2012_04
ORD IDord-88acc85fdf57428c9d42bff593e1e905
출처 메모uspto-grants-2012_04