Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → Methyl 4-(1-methylethoxy)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 4-Isopropoxybenzoic acid | HCID 72972 | — |
| 생성물 | Methyl 4-(1-methylethoxy)benzoate | HCID 3015807 | 67% |
반응 단계
3.0 g of 4-isopropoxy-benzoic acid (16.7 mmol, 1.0 eq) were dissolved in MeOH (20 mL) and a catalytic quantity of sulfuric acid was added; the mixture was heated at reflux for 2 days. The solvent was then evaporated and the residue was dissolved in DCM and washed with 10% NaOH. The organic phases were dried and evaporated to give 2.2 g of title product (yield 67%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08163729B2 |
| 출처 데이터셋 | uspto-grants-2012_04 |
| ORD ID | ord-88acc85fdf57428c9d42bff593e1e905 |
| 출처 메모 | uspto-grants-2012_04 |