Methyl 3-(2-chlorophenyl)propanoate → 3-(2-Chlorophenyl)propanoic acid

HRID 1701338

반응식

HRID 1701338 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][C:10]([O:12]C)=[O:11]>[OH-].[Na+]>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][C:10]([OH:12])=[O:11]

참가 물질

3

반응물 1

HCID 18913495Methyl 3-(2-chlorophenyl)propanoate

생성물 1

HCID 956763-(2-Chlorophenyl)propanoic acid

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매

실험 절차

Methyl 3-(2-chlorophenyl)propionate was refluxed in 10% aqueous sodium hydroxide (1 l.) for two hours and the reaction mixture was cooled, acidified and filtered. The filter cake was dissolved in hot aqueous sodium bicarbonate and filtered. The filtrate was acidified and filtered to yield 3-(2-chlorophenyl)propionic acid.

후처리

  1. temperaturethe reaction mixture was cooled
  2. filtrationfiltered
  3. dissolutionThe filter cake was dissolved in hot aqueous sodium bicarbonate
  4. filtrationfiltered
  5. filtrationfiltered

출처 및 근거

ORD 기록
ord-50b52fd89ee74f889f0ab0f9aeecf7b9
출처 데이터셋
uspto-grants-1980_03
특허 번호
US04192888

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