Potassium Carbonate → HCID 54035734, 화합물
반응식
[C:1]1([OH:11])[C:10]2[CH2:9][CH2:8][CH2:7][CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.C(=O)([O-])[O-].[K+].[K+].Br[CH2:19][C:20]([O:22][CH3:23])=[O:21]>CC(=O)CC>[C:1]1([O:11][CH2:19][C:20]([O:22][CH3:23])=[O:21])[C:10]2[CH2:9][CH2:8][CH2:7][CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1참가 물질
5
실험 절차
10 g 5,6,7,8-tetrahyro-1-naphthol are dissolved in 150 ml 2-butanone and then 18.5 g potassium carbonate and 12.3 g methyl bromoacetate are introduced into the mixture. After having been refluxed for 24 hours, the mixture is filtered, the solvent evaporated under reduced pressure and after removal of the starting phenol soluble in aqueous basic medium, 13.1 g of final product are distilled.
후처리
- temperatureAfter having been refluxed for 24 hours
- filtrationthe mixture is filtered
- customthe solvent evaporated under reduced pressure
- customafter removal of the starting phenol soluble in aqueous basic medium, 13.1 g of final product
- distillationare distilled
출처 및 근거
- ORD 기록
- ord-6cd91dddd17f4838aca575df6b89fc97
- 출처 데이터셋
- uspto-grants-1980_03
- 특허 번호
- US04195093
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