Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → 7-(3-Ethyl-4.5-diphenyl-2-oxo-4-imidazolin-1-yl) enanthic acid ethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | Ethyl 7-chloroheptanoate | HCID 529988 | — |
| 반응물 | 1-ethyl-4,5-diphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 12675126 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 7-(3-Ethyl-4.5-diphenyl-2-oxo-4-imidazolin-1-yl) enanthic acid ethyl ester | HCID 53708715 | — |
반응 단계
The product is obtained as described in example 1 from 2.1 g of NaH (80% suspension in mineral oil), 18.5 g of 1-ethyl-4.5-diphenyl-4-imidazolin-2-one, 140 cc. of DMF, 13.5 g of 7-chloroenanthic acid ethyl ester and 2.1 g of NaJ.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04349684 |
| 출처 데이터셋 | uspto-grants-1982_09 |
| ORD ID | ord-5c9d7533d6a6403cad679228344b1a0a |
| 출처 메모 | uspto-grants-1982_09 |