Hydrochloric Acid → 5-(Chloromethyl)uracil

HRID 1703050

반응식

HRID 1703050 반응식
O[CH2:2][C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1.[ClH:11]>>[Cl:11][CH2:2][C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1

참가 물질

3

실험 절차

A solution of 1.4 g. (0.010 mole) of 5-hydroxymethyl uracil in 12.5 ml. of concentrated hydrochloric acid was prepared. A colorless precipitate (5-chloromethyl uracil) formed within two minutes and after about ten minutes the precipitate was collected by filtration, washed rapidly with ice cold water, dried and then suspended in 10 ml. of dimethylformamide.

출처 및 근거

ORD 기록
ord-4dcebf16c68b4e21871e38c7da8478f6
출처 데이터셋
uspto-grants-1982_09
특허 번호
US04350754

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