Hydrazinecarboxylic acid, ethyl ester → HCID 135981644, 화합물

반응식

[CH3:1][C:2]1[NH:3][C:4]([CH3:9])=[C:5]([CH:7]=O)[N:6]=1.[C:10]([O:14][CH2:15][CH3:16])(=[O:13])[NH:11][NH2:12]>>[CH2:15]([O:14][C:10](=[O:13])[NH:11][N:12]=[CH:7][C:5]1[N:6]=[C:2]([CH3:1])[NH:3][C:4]=1[CH3:9])[CH3:16]

참가 물질

반응물 2

HCID 20064Hydrazinecarboxylic acid, ethyl ester

HCID 132064322,5-Dimethyl-1H-imidazole-4-carbaldehyde

생성물 1

HCID 135981644HCID 135981644, 화합물

실험 절차

A 6.2 gm. portion of 2,5-dimethyl-4-imidazolecarboxaldehyde and 6.24 gm. of ethyl carbazate are reacted as described in Example 32 giving the desired product, m.p. 207.5°-210° C. (resolidifies 248°-252° C.).

출처 및 근거

ORD 기록: ord-836fdf44ad964e10a0ad160139f18d1b
출처 데이터셋: uspto-grants-1978_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04124766

반응 노트

불러오는 중…