2,3-Dihydroxybutanedioic Acid → Dilithium tartrate

반응식

[C:1]([OH:10])(=[O:9])[CH:2]([CH:4]([C:6]([OH:8])=[O:7])[OH:5])[OH:3].[OH-].[Li+:12]>O>[C:1]([O-:10])(=[O:9])[CH:2]([CH:4]([C:6]([O-:8])=[O:7])[OH:5])[OH:3].[Li+:12].[Li+:12]

참가 물질

실험 절차

Tartaric acid (15.0 g, 0.1 mole) is dissolved in 40 ml. water and treated with lithium hydroxide (8.4 g, 0.2 mole). The resulting solution is evaporated to a small volume under reduced pressure and the residue is treated with p-dioxane. The resulting precipitate is filtered and dried under vacuum to give the di-lithium tartarate (17.7 g).

후처리

customThe resulting solution is evaporated to a small volume under reduced pressure
additionthe residue is treated with p-dioxane
filtrationThe resulting precipitate is filtered
customdried under vacuum

출처 및 근거

ORD 기록: ord-62ef0fe86dd54de989a2783046eb179e
출처 데이터셋: uspto-grants-1980_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04208422

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참가 물질

반응물 2

HCID 8752,3-Dihydroxybutanedioic Acid

HCID 3939Lithium Hydroxide

생성물 1

HCID 10176260Dilithium tartrate수율 109.3%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

후처리

customThe resulting solution is evaporated to a small volume under reduced pressure
additionthe residue is treated with p-dioxane
filtrationThe resulting precipitate is filtered
customdried under vacuum

출처 및 근거

ORD 기록: ord-62ef0fe86dd54de989a2783046eb179e
출처 데이터셋: uspto-grants-1980_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04208422

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불러오는 중…