Benzoyl chloride → HCID 18963390, 화합물

반응식

[C:1]([C:4]1[CH2:9][CH2:8][CH2:7][NH:6][CH:5]=1)(=[O:3])[CH3:2].[C:10](Cl)(=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:10]([N:6]1[CH2:7][CH2:8][CH2:9][C:4]([C:1]([CH3:2])=[O:3])=[CH:5]1)(=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

참가 물질

반응물 2

HCID 7412Benzoyl chloride

HCID 32845951-(1,4,5,6-Tetrahydropyridin-3-yl)ethanone

생성물 1

HCID 18963390HCID 18963390, 화합물

실험 절차

Methyl 1-benzoyl-1,4,5,6-tetrahydro-3-pyridyl ketone was prepared from 3-acetyl-1,4,5,6-tetrahydropyridine and benzoyl chloride according to the procedure of Part b) of Example 1. The product was recrystallised from ethanol/water m.pt. 93°-95° C.

후처리

customThe product was recrystallised from ethanol/water m.pt. 93°-95° C.

출처 및 근거

ORD 기록: ord-fd6ec49b771345388e5b20cdd6d2dea8
출처 데이터셋: uspto-grants-1994_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05352793

반응 노트

불러오는 중…