Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Aminobenzoic Acid → Carbamazepine 4-aminobenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Aminobenzoic Acid | HCID 978 | — |
| 반응물 | Carbamazepine | HCID 2554 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Carbamazepine 4-aminobenzoic acid | HCID 68425507 | — |
반응 단계
40 mg (0.1693 mmol) of carbamazepine and 30 mg (0.1421 mmol) of 4-aminobenzoic acid were dissolved in approximately 3 mL methanol. Slow evaporation of the solvent yielded clear plates of carbamazepine:4-aminobenzoic acid (2:1) co-crystal. The co-crystal was analyzed via IR spectroscopy and single-crystal x-ray diffraction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07803786B2 |
| 출처 데이터셋 | uspto-grants-2010_09 |
| ORD ID | ord-44bb3b9cb73747d187051a5a3f9e2af5 |
| 출처 메모 | uspto-grants-2010_09 |