Benzoyl Peroxide → 2-Ethylhexyl methacrylate-giycidyl methacrylate

HRID 1728533

반응식

HRID 1728533 반응식
[C:1]([O:6][CH2:7][CH:8]([CH2:13][CH3:14])[CH2:9][CH2:10][CH2:11][CH3:12])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:15]([O:20][CH2:21][CH:22]1[O:24][CH2:23]1)(=[O:19])[C:16]([CH3:18])=[CH2:17].C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>>[CH2:21]([O:20][C:15](=[O:19])[C:16]([CH3:18])=[CH2:17])[CH:22]1[O:24][CH2:23]1.[C:1]([O:6][CH2:7][CH:8]([CH2:13][CH3:14])[CH2:9][CH2:10][CH2:11][CH3:12])(=[O:5])[C:2]([CH3:4])=[CH2:3]

참가 물질

4

반응물 3

HCID 7187Benzoyl PeroxideHCID 7837Glycidyl methacrylateHCID 127132-Ethylhexyl methacrylate

생성물 1

HCID 867479712-Ethylhexyl methacrylate-giycidyl methacrylate

반응 조건

온도
90 °C

실험 절차

To the above solvent, a mixture of 200 g of 2-ethylhexyl methacrylate, 10 g of glycidyl methacrylate and 2 g of benzoyl peroxide was added dropwise at a constant speed over a period of 2 hours, followed by stirring at 90° C. for 4 hours to complete the polymerization reaction. Thus, 2-ethylhexyl methacrylate - giycidyl methacrylate copolymer was obtained.

후처리

  1. additionwas added dropwise at a constant speed over a period of 2 hours
  2. customthe polymerization reaction

출처 및 근거

ORD 기록
ord-d9b15d8727d74cf885b73d8610e98b6b
출처 데이터셋
uspto-grants-1994_07
특허 번호
US05328794

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