Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → 1-Methyl-2-[[[4-(tetradecyloxy)benzoyl]amino]methyl]pyridinium iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | N-(2-Pyridinylmethyl)-4-(tetradecyloxy)benzamide | HCID 10093859 | — |
| 생성물 | 1-Methyl-2-[[[4-(tetradecyloxy)benzoyl]amino]methyl]pyridinium iodide | HCID 10076647 | — |
반응 단계
A mixture of 1.0 g of product from Example 4 and 7.33 ml of methyl iodide is heated, in a dark sealed tube, at 100°-120° C. for 22 hours. The cooled reaction mixture is concentrated in vacuo and recrystallized 2 times from methyl alcohol to give 1.15 g of the desired product as light yellow microneedles.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05328921 |
| 출처 데이터셋 | uspto-grants-1994_07 |
| ORD ID | ord-48a865b3a6d7484386a91d71f8746edd |
| 출처 메모 | uspto-grants-1994_07 |