1-Phenylcyclohexane-1-carboxylic acid → Methyl 1-phenylcyclohexane-1-carboxylate

HRID 1729067

반응식

HRID 1729067 반응식
[C:1]1([C:7]2([C:13]([OH:15])=[O:14])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:16]OC(C1CCCC1)=O>CCOCC>[CH3:16][O:14][C:13]([C:7]1([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)=[O:15]

참가 물질

4

반응물 2

HCID 708171-Phenylcyclohexane-1-carboxylic acidHCID 78365Methyl cyclopentanecarboxylate

생성물 1

HCID 15105202Methyl 1-phenylcyclohexane-1-carboxylate

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

This compound was prepared (1.91 g, 8.76 mmol, 89%) from the product of Step A (2.00 g, 9.8 mmol) following the procedure for synthesis of methyl-1-cyclopentanecarboxylate as set forth in Step A, Example 1. The product of this step was homogeneous by TLC (ether:C2Cl2, 2:1) and used in the next step without further purification. CIMS 219 m/z (M+1).

후처리

  1. customused in the next step without further purification

출처 및 근거

ORD 기록
ord-a3d1cba68a344dc4abd002d70273a898
출처 데이터셋
uspto-grants-1994_07
특허 번호
US05331010

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