Ethylamine → 4-Ethylamino-3-nitrobenzamide

HRID 1729581

반응식

HRID 1729581 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1Cl)[C:7]([NH2:9])=[O:8])([O-:3])=[O:2].[CH2:14]([NH2:16])[CH3:15]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[NH:16][CH2:14][CH3:15])[C:7]([NH2:9])=[O:8])([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 6341EthylamineHCID 279424-Chloro-3-nitrobenzamide

생성물 1

HCID 37089224-Ethylamino-3-nitrobenzamide

실험 절차

II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).

후처리

  1. temperatureThe mixture was cooled
  2. customthe precipitate was collected
  3. customcrystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product)

출처 및 근거

ORD 기록
ord-bb3097a7e15a44488e01fcb467723d81
출처 데이터셋
uspto-grants-1976_11
특허 번호
US03989522

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