Ammonia → N,N-Dimethylaminopropyl acrylamide

HRID 1732222

반응식

O[CH2:2][CH2:3][C:4]([NH2:6])=[O:5].[CH3:7][N:8]([CH3:13])[CH2:9][CH2:10][CH2:11]N.N.[OH-].[Na+]>>[CH3:7][N:8]([CH3:13])[CH2:9][CH2:10][CH2:11][NH:6][C:4](=[O:5])[CH:3]=[CH2:2]

참가 물질

반응물 4

HCID 222Ammonia

HCID 7993N,N-Dimethyl-1,3-propanediamine

HCID 14798Sodium Hydroxide

HCID 41451403-Hydroxypropanamide

생성물 1

HCID 77452N,N-Dimethylaminopropyl acrylamide

실험 절차

59.3 g of β-hydroxypropionic acid amide and 68 g of 3-dimethylaminopropylamine were heated for 5 hours in a temperature range of 125°-168° C. until the evolution of ammonia was complete. After adding 1 g of pulverised sodium hydroxide the reaction mixture was distilled.

후처리

distillationwas distilled

출처 및 근거

ORD 기록: ord-9fb2048b1977420aad17c78493b3ea51
출처 데이터셋: uspto-grants-1980_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04237067

연결된 노트

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