Hydrogen Bromide → HCID 12717836, 화합물

HRID 1732846노트

반응식

HRID 1732846 반응식
[N:1]12C[N:5]3[CH2:6][P:7]([CH2:9][N:3](C3)C1)[CH2:8]2.[BrH:11]>O>[BrH:11].[BrH:11].[BrH:11].[NH2:5][CH2:6][P:7]([CH2:9][NH2:3])[CH2:8][NH2:1]

참가 물질

4

반응물 2

HCID 260Hydrogen BromideHCID 1430611,3,5-Triaza-7-phosphaadamantane

생성물 1

HCID 12717836HCID 12717836, 화합물수율 74.2%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Following the procedure outline in Example 6, 3.14 g (0.02 mol) of 1,3,5-triaza-7-phosphaadamantane was hydrolyzed with a solution of 25 g (0.15 mol) of 48% hydrobromic acid and 40 g of water, giving, after workup, 5.4 g (74% yield) of tris(aminomethyl)phosphine trihydrobromide as a white, crystalline solid, dec. 214° C. without melting.

후처리

  1. customgiving

출처 및 근거

ORD 기록
ord-db44294a14f94cf4ad30e2fb78667ef7
출처 데이터셋
uspto-grants-1980_12
특허 번호
US04239701

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