Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Toluene → Propazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | 1,1,1-Trichloroethane | HCID 6278 | — |
| 반응물 | HCID 19438222 | HCID 19438222 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | Propazine | HCID 4937 | 12% |
반응 단계
Similar reactions, in which 1,1,1-trichloroethane (reflux 75° C.) and 1,4-dioxan (reflux 105° C.) were used as solvents instead of toluene, both gave diethyl 2,4-bis(isopropylamino)-1,3,5-triazine-6-phosphonate in 81% yield, together with 2-chloro-4,6-bis(isopropylamino)-1,3,5-triazine (yield 12-17%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05534573 |
| 출처 데이터셋 | uspto-grants-1996_07 |
| ORD ID | ord-e3aaf468c36b4760b98f8dcc8acce084 |
| 출처 메모 | uspto-grants-1996_07 |