Hydrogen Bromide → HCID 68449648, 화합물

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C[O:2][C:3]1[N:8]=[C:7]([CH:9]([NH2:11])[CH3:10])[CH:6]=[CH:5][CH:4]=1.[BrH:12]>>[BrH:12].[NH2:11][CH:9]([C:7]1[NH:8][C:3](=[O:2])[CH:4]=[CH:5][CH:6]=1)[CH3:10]

참가 물질

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HCID 260Hydrogen Bromide

HCID 594786346-Methoxy-alpha-methyl-2-pyridinemethanamine

생성물 1

HCID 68449648HCID 68449648, 화합물

반응 조건

온도: 80 °C

실험 절차

To 1.6 g of 1-(6-methoxypyridin-2-yl)ethanamine was added 23.7 ml of a 47% aqueous hydrobromic acid solution, followed by stirring at 80° C. for 60 hours. After evaporating the solvent under reduced pressure, the residue was washed with diethyl ether to obtain 2.95 g of 6-(1-aminoethyl)pyridin-2(1H)-one hydrobromide as a pale brown solid.

후처리

customAfter evaporating the solvent under reduced pressure
washthe residue was washed with diethyl ether

출처 및 근거

ORD 기록: ord-17331e8b08434e0ca835fc01a2eb1b37
출처 데이터셋: uspto-grants-2015_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US09150541B2

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