1-Methylimidazole → HCID 131719089, 화합물

반응식

C(=O)([O-])[O-].[Co+2:5].[CH:6](=[O:14])[C:7]1[C:8](=[CH:10][CH:11]=[CH:12][CH:13]=1)[OH:9].[CH3:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1>>[CH3:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1.[CH3:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1.[Co+2:5].[CH:6](=[O:14])[C:7]1[C:8](=[CH:10][CH:11]=[CH:12][CH:13]=1)[OH:9].[CH:6](=[O:14])[C:7]1[C:8](=[CH:10][CH:11]=[CH:12][CH:13]=1)[OH:9]

참가 물질

반응물 3

HCID 13901-Methylimidazole

HCID 6998Salicylaldehyde

HCID 10565Cobaltous carbonate

생성물 1

HCID 131719089HCID 131719089, 화합물수율 97%

실험 절차

1 mole of cobalt (II) carbonate was thoroughly mixed with 2 moles of salicylaldehyde with an excess of 1-methyl imidazole at moderate temperatures using the procedure of Example 1 to obtain a 97% yield of bis-(salicylaldehyde)-cobalt (II) di(1-methylimidazole)

출처 및 근거

ORD 기록: ord-ae1f7ea938cc4857adccff19448cce16
출처 데이터셋: uspto-grants-1995_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05444030

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