Potassium Carbonate → HCID 19858315, 화합물

HRID 1762129노트

반응식

HRID 1762129 반응식
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

생성물 1

HCID 19858315HCID 19858315, 화합물

시약·촉매·용매 1

HCID 24813Phosphorus oxychloride촉매

실험 절차

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and was concentrated to obtain the product as an oil.

후처리

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationwas concentrated

출처 및 근거

ORD 기록
ord-42518c203af64540aaafefcd08cba9c2
출처 데이터셋
uspto-grants-1989_05
특허 번호
US04831035

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