Diazomethane → HCID 3864057, 화합물

HRID 1763758노트

반응식

HRID 1763758 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]([CH2:13][C:14]([OH:16])=[O:15])[CH3:12])(=[O:10])=[O:9])=[CH:4][CH:3]=1.[N+](=[CH2:19])=[N-]>>[CH3:19][O:15][C:14](=[O:16])[CH2:13][N:11]([S:8]([C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=1)(=[O:9])=[O:10])[CH3:12]

참가 물질

3

반응물 2

HCID 9550DiazomethaneHCID 362744(4-Chloro-benzenesulfonyl)-methyl-amino]-acetic acid

생성물 1

HCID 3864057HCID 3864057, 화합물

실험 절차

2 Parts of N-p-chlorobezenesulfonyl-sarcosine is added to a diazomethane-ethereal solution. After the generation of nitrogen has ceased, the precipitated reaction product is collected by filtration to obtain 1.2 parts of N-p-chlorobenzenesulfonyl-sarcosine methyl ester, m.p. 80°-80.5° C.

후처리

  1. customthe precipitated reaction product
  2. filtrationis collected by filtration

출처 및 근거

ORD 기록
ord-3a77f8aa4e684fd795cec1c2c1a463bf
출처 데이터셋
uspto-grants-1978_09
특허 번호
US04113463

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