Hydrochloric Acid → HCID 22770497, 화합물

HRID 1764097노트

반응식

HRID 1764097 반응식
[CH3:1][N:2]([CH3:20])[C:3]1[CH:8]=[C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:6]=[C:5]2[N:15]([CH3:19])[N:16]=[C:17]([CH3:18])[C:4]=12.[ClH:21]>C(O)C>[ClH:21].[CH3:20][N:2]([CH3:1])[C:3]1[CH:8]=[C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:6]=[C:5]2[N:15]([CH3:19])[N:16]=[C:17]([CH3:18])[C:4]=12

참가 물질

4

반응물 2

HCID 313Hydrochloric Acid2회HCID 227704984-Dimethylamino-1,3-dimethyl-6-phenyl-1H-pyrazolo[3,4-b]pyridine

생성물 1

HCID 22770497HCID 22770497, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

To 16.5 gms. of 4-dimethylamino-1,3-dimethyl-6-phenyl-1H-pyrazolo[3,4-b]pyridine (0.062 mol.) dissolved in 250 ml. of absolute ethanol, 10.7 ml. of ethereal hydrochloric acid (228 gms/1) are added. The solution is allowed to crystallize overnight to obtain 17.2 gms. (91%) of the hydrochloride, m.p. 219°-220° C. (dec.)

후처리

  1. customto crystallize overnight
  2. customto obtain 17.2 gms

출처 및 근거

ORD 기록
ord-30dacc8d721e458b97c5283bc628b71e
출처 데이터셋
uspto-grants-1978_09
특허 번호
US04115394

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