Diazomethane → Methyl-4-iodocinnamate

HRID 1765697노트

반응식

HRID 1765697 반응식
[I:1][C:2]1[CH:12]=[CH:11][C:5]([CH:6]=[CH:7][C:8]([OH:10])=[O:9])=[CH:4][CH:3]=1.[N+](=[CH2:15])=[N-]>CO.C(OCC)C>[CH3:15][O:9][C:8](=[O:10])[CH:7]=[CH:6][C:5]1[CH:4]=[CH:3][C:2]([I:1])=[CH:12][CH:11]=1

참가 물질

5

반응물 2

HCID 9550DiazomethaneHCID 35997884-Iodocinnamic acid

생성물 1

HCID 582796Methyl-4-iodocinnamate

시약·촉매·용매 2

HCID 887Methanol용매HCID 3283Diethyl Ether용매

실험 절차

A stirred, cooled (ice bath) solution of 4-iodo-cinnamic Acid in methanol was treated with a solution of diazomethane in diethyl ether. The reaction mixture was allowed to warm to ambient temperature, the volatiles were-evaporated in vacuo to afford the title compound.

후처리

  1. customthe volatiles were-evaporated in vacuo

출처 및 근거

ORD 기록
ord-885fbbbe44cf4bea960f63f23abe9bbc
출처 데이터셋
uspto-grants-2007_06
특허 번호
US07226951B2

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