Hydrochloric Acid → (2E)-2-methoxyimino-N-methyl-2-(2-phenoxyphenyl)acetamide
반응식
[CH3:1][O:2]/[N:3]=[C:4](/[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[O:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)\[C:5]([NH:7][CH3:8])=[O:6].Cl>CO>[CH3:1][O:2]/[N:3]=[C:4](\[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[O:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)/[C:5]([NH:7][CH3:8])=[O:6]참가 물질
4
실험 절차
To Z-2-methoxyimino-N-methyl-2-(2phenoxyphenyl)acetamide VI" (0.28 g, 1.0 mmole) were added dried methanol (3 ml) and 10% hydrochloric acid solution in methanol (0.36 g, 1.0 mmole) and the mixture was heated under reflux for 6 hours to conduct isomerization.
후처리
- temperaturethe mixture was heated
- temperatureunder reflux for 6 hours
출처 및 근거
- ORD 기록
- ord-4192ae6a7b1045aebb00bd10cd1a198d
- 출처 데이터셋
- uspto-grants-1995_01
- 특허 번호
- US05380913
반응 노트
불러오는 중…