1-Bromopropane → HCID 178462650, 화합물

HRID 1774325노트

반응식

HRID 1774325 반응식
[CH3:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[CH:4][C:3]=1[N:9]1[CH:13]=[CH:12][N:11]=[CH:10]1.[Br:14][CH2:15][CH2:16]C>C1COCC1>[Br-:14].[CH2:15]([N:11]1[CH:12]=[CH:13][N+:9]([C:3]2[CH:4]=[CH:5][C:6]([CH3:8])=[CH:7][C:2]=2[CH3:1])=[CH:10]1)[CH3:16]

참가 물질

4

반응물 2

HCID 78401-BromopropaneHCID 101301771-(2,4-Dimethylphenyl)-1H-imidazole

생성물 1

HCID 178462650HCID 178462650, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

According to the general synthesis procedure, 2.91 mmol (0.500 g) 1-(2,4-dimethylphenyl)imidazole and 3.20 mmol (0.392 g) 1-bromopropane are dissolved in 5 ml THF and heated for 6 h to 120° C.

후처리

  1. temperatureheated for 6 h to 120° C.

출처 및 근거

ORD 기록
ord-a6a4614a3c9a4c5ab4c88be7c3284228
출처 데이터셋
uspto-grants-2016_02
특허 번호
US09260397B2

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