1-Bromopropane → 1-(4-Chlorophenyl)-3-propyl imidazolium bromide

HRID 1774332

반응식

HRID 1774332 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)=[CH:4][CH:3]=1.[Br:13][CH2:14][CH2:15][CH3:16]>C1COCC1>[Br-:13].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N+:8]2[CH:12]=[CH:11][N:10]([CH2:14][CH2:15][CH3:16])[CH:9]=2)=[CH:6][CH:7]=1

참가 물질

4

반응물 2

HCID 78401-BromopropaneHCID 1428591-(4-Chlorophenyl)-1H-imidazole

생성물 1

HCID 1784563371-(4-Chlorophenyl)-3-propyl imidazolium bromide

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

According to the general synthesis procedure, 5.60 mmol (1.00 g) 1-(4-chlorophenyl)imidazole and 6.7 mmol (0.830 g, 0.61 ml) 1-bromopropane are dissolved in 5 ml THF and heated for 18.5 h to 90° C.

후처리

  1. temperatureheated for 18.5 h to 90° C.

출처 및 근거

ORD 기록
ord-cf7ca4f689104a3e9d7cb59b41ee48eb
출처 데이터셋
uspto-grants-2016_02
특허 번호
US09260397B2

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