Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Myristyl bromide → 1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Myristyl bromide | HCID 8208 | — |
| 반응물 | 1-(4-Chlorophenyl)-1H-imidazole | HCID 142859 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromide | HCID 178443152 | — |
반응 단계
According to the general synthesis procedure 5.6 mmol (1.00 g) 1-(4-chlorophenyl)imidazole and 6.7 mmol (1.86 g, 1.82 ml) 1-bromotetradecane are dissolved in 5 ml THF and heated for 42 h to 90° C. At the end of the reaction the reaction mixture is cooled down to room temperature and the product is precipitated with diethylether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09260397B2 |
| 출처 데이터셋 | uspto-grants-2016_02 |
| ORD ID | ord-102dde7402434d619b8f589ac226a8b0 |
| 출처 메모 | uspto-grants-2016_02 |