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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Chloroform → HCID 86641263, 화합물

HRID 1779129
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HRID 1779129 반응식
[CH2:1]([N:9]1[C:13](=[O:14])[CH:12]=[CH:11][C:10]1=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:16]1(=[O:22])[O:21][C:19](=[O:20])[CH:18]=[CH:17]1.COC(=O)C(N=NC(C)(C)C(OC)=O)(C)C.C(Cl)(Cl)Cl>CO>[CH2:1]([N:9]1[C:10](=[O:15])[CH:11]=[CH:12][C:13]1=[O:14])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[C:19]1(=[O:20])[O:21][C:16](=[O:22])[CH:17]=[CH:18]1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 4

HCID 6212ChloroformHCID 7923Maleic AnhydrideHCID 757631,1'-Dimethyl 2,2'-(1,2-diazenediyl)bis(2-methylpropanoate)HCID 512829Octyl Maleimide

생성물 1

HCID 86641263HCID 86641263, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Into a sealed glass tube were introduced 26 g of N-n-octylmaleimide, 4.8 g of maleic anhydride, and 0.04 g of dimethyl-2,2′-azobisisobutyrate as a polymerization initiator. After nitrogen displacement, a radical polymerization reaction was conducted under the conditions of a polymerization temperature of 60° C. and a polymerization time of 5 hours. Chloroform was added after the reaction to obtain a polymer solution. Thereafter, this solution was mixed with excess methanol to thereby precipitate the polymer. The polymer obtained was taken out by filtration, subsequently sufficiently washed with methanol, and dried at 80° C. Thus, an N-n-octylmaleimide-maleic anhydride copolymer resin was obtained in an amount of 18 g. The N-n-octylmaleimide-maleic anhydride copolymer resin obtained contained maleic anhydride residue unit in an amount of 20% by weight and had a number-average molecular weight of 140,000.

후처리

  1. customAfter nitrogen displacement, a radical polymerization reaction
  2. customwas conducted under the conditions of a polymerization temperature of 60° C.
  3. customa polymerization time of 5 hours
  4. customafter the reaction
  5. customto obtain a polymer solution
  6. customto thereby precipitate the polymer
  7. customThe polymer obtained
  8. filtrationwas taken out by filtration
  9. washsubsequently sufficiently washed with methanol
  10. customdried at 80° C

출처 및 근거

ORD 기록
ord-5197b615fbef4353a3f2001899ca19f6
출처 데이터셋
uspto-grants-2016_02
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US09268076B2

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