Piperonyl alcohol → 5-(Benzo[1,3]dioxol-5-ylmethoxy)-2-(4-octyloxyphenyl)pyrimidine

HRID 1779267노트

반응식

HRID 1779267 반응식
[CH2:1]([O:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[N:21]=[CH:20][C:19]([OH:22])=[CH:18][N:17]=2)=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[O:23]1[C:27]2[CH:28]=[CH:29][C:30]([CH2:32]O)=[CH:31][C:26]=2[O:25][CH2:24]1>>[O:23]1[C:27]2[CH:28]=[CH:29][C:30]([CH2:32][O:22][C:19]3[CH:18]=[N:17][C:16]([C:13]4[CH:14]=[CH:15][C:10]([O:9][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])=[CH:11][CH:12]=4)=[N:21][CH:20]=3)=[CH:31][C:26]=2[O:25][CH2:24]1

참가 물질

3

반응물 2

HCID 10322Piperonyl alcoholHCID 144963952-(4-(Octyloxy)phenyl)pyrimidin-5-ol

생성물 1

HCID 190503395-(Benzo[1,3]dioxol-5-ylmethoxy)-2-(4-octyloxyphenyl)pyrimidine

실험 절차

By Mitsunobu etherification of 2-(4-octyloxyphenyl)pyrimidin-5-ol using benzo[1,3]dioxol-5-ylmethanol analogously to Example 208.

출처 및 근거

ORD 기록
ord-39971bb73de9472592589765cb806cac
출처 데이터셋
uspto-grants-1997_05
특허 번호
US05626791

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