2,4-Dichlorobenzonitrile → (2,4-Dichlorophenyl)(phenyl)methanamine

HRID 1782047

반응식

HRID 1782047 반응식
[Cl:1][C:2]1[CH:9]=[C:8]([Cl:10])[CH:7]=[CH:6][C:3]=1[C:4]#[N:5].[C:11]1([Mg]Br)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.[BH4-].[Na+]>CO>[Cl:1][C:2]1[CH:9]=[C:8]([Cl:10])[CH:7]=[CH:6][C:3]=1[CH:4]([NH2:5])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

참가 물질

5

반응물 3

HCID 810502,4-DichlorobenzonitrileHCID 4311764Sodium borohydrideHCID 178418255HCID 178418255, 화합물

생성물 1

HCID 43184805(2,4-Dichlorophenyl)(phenyl)methanamine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The title compound was prepared from 2,4-dichloro benzonitrile and a) phenyl magnesium bromide b) NaBH4 in MeOH in analogy to known methods.9

출처 및 근거

ORD 기록
ord-096b44d1e51a4d24bf466367fbbf57f7
출처 데이터셋
uspto-grants-2009_03
특허 번호
US07498339B2

연결된 노트

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