Nitric Acid → HCID 178469037, 화합물
반응식
[CH2:1]([O:3][C:4](=[O:12])[C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[CH:7][CH:6]=1)[CH3:2].[N+:13]([O-:16])([OH:15])=[O:14].[N:17]#[C:18][NH2:19]>C(O)C>[N+:13]([O-:16])([OH:15])=[O:14].[CH2:1]([O:3][C:4](=[O:12])[C:5]1[CH:10]=[CH:9][C:8]([NH:11][C:18]([NH2:19])=[NH:17])=[CH:7][CH:6]=1)[CH3:2]참가 물질
5
실험 절차
4-aminobenzoic acid ethyl ester (20 g, 0.121 mol), nitric acid (7.26 g, 0.121 mol), cyanamide (50%, 14 ml 0.182 mol) were mixed under reflux with ethanol (50 ml). After 24 hr, the mixture was cooled to RT, and then washed with ethanol to give the titled compound as crystalline solid.
후처리
- washwashed with ethanol
출처 및 근거
- ORD 기록
- ord-c391bf99df534663a7c96a7ab4abfa3f
- 출처 데이터셋
- uspto-grants-2009_03
- 특허 번호
- US07501424B2
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