Sodium Bicarbonate → Sodium

HRID 1788622노트

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HRID 1788622 반응식
[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[CH:6][C:5]=1CCC(O)=O)([O-:3])=[O:2].[Na:18].C(=O)([O-])O.[Na+].NC1C=C(N)C=CC=1[O:27][CH:28]([CH3:32])[C:29]([OH:31])=[O:30]>>[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[CH:6][C:5]=1[O:27][CH:28]([CH3:32])[C:29]([OH:31])=[O:30])([O-:3])=[O:2].[Na:18]

참가 물질

6

반응물 4

HCID 516892Sodium BicarbonateHCID 27505133-(2,4-dinitrophenyl)propanoic AcidHCID 5360545Sodium2회HCID 20189859HCID 20189859, 화합물

생성물 2

HCID 5360545SodiumHCID 20189861HCID 20189861, 화합물

실험 절차

The 2-(2,4-dinitrophenoxy)-propionic acid from step (a) was converted into the sodium salt with sodium hydrogen carbonate and reduced in aqueous solution, using procedures analogous to those set forth in A, and the sodium salt was then isolated. Five grams of 2-(2,4-dinitrophenoxy)-propionic acid yielded 2.4 gm of sodium salt of 2-(2,4-diaminophenoxy)-propionic acid.

후처리

  1. customwas then isolated

출처 및 근거

ORD 기록
ord-0ace83c6371546509178e06bffa6169c
출처 데이터셋
uspto-grants-1987_08
특허 번호
US04684371

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