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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Water → HCID 12257138, 화합물

HRID 1788748
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HRID 1788748 반응식
[CH:1]1[CH2:5][CH2:4][CH2:3][CH:2]=1.[N+]([O-])([O-])=O.[Hg+2:10].[N+]([O-])([O-])=O.[Cl-:15].[Na+].[OH2:17].[C:18](#[N:20])[CH3:19]>>[C:18]([NH:20][C@@H:1]1[CH2:5][CH2:4][CH2:3][C@H:2]1[Hg:10][Cl:15])(=[O:17])[CH3:19]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 5

HCID 962WaterHCID 5234Sodium ChlorideHCID 6342Acetonitrile2회HCID 8882CyclopenteneHCID 24864Mercuric nitrate

생성물 1

HCID 12257138HCID 12257138, 화합물

실험 절차

10 ml of cyclopentene in 30 ml of acetonitrile are added dropwise to a suspension of 38.3 g of mercury(II) nitrate in 80 ml of acetonitrile at 0° C. After 1 hour at room temperature, the mixture is poured into a mixture of 60 ml of saturated sodium chloride solution and 250 ml of water, and the solid is filtered off with suction, washed with water and dried. 26 g of the title compound are obtained as an amorphous powder.

후처리

  1. filtrationthe solid is filtered off with suction
  2. washwashed with water
  3. customdried

출처 및 근거

ORD 기록
ord-56e3c6cb28d240338fbb6e5b190866bb
출처 데이터셋
uspto-grants-1987_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04684662

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