Ethyl orthoformate → HCID 13958430, 화합물

HRID 1789427노트

반응식

HRID 1789427 반응식
[NH2:1][C:2]1[CH:3]=[N:4][C:5]2[C:10]([C:11]=1[NH:12][CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:9][CH:8]=[CH:7][CH:6]=2.[CH:21](OCC)(OCC)OCC>C(O)=O>[C:15]1([CH2:14][CH2:13][N:12]2[C:11]3[C:10]4[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=4[N:4]=[CH:3][C:2]=3[N:1]=[CH:21]2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

참가 물질

4

반응물 2

HCID 31214Ethyl orthoformateHCID 20183591HCID 20183591, 화합물

생성물 1

HCID 13958430HCID 13958430, 화합물

시약·촉매·용매 1

HCID 284Formic Acid용매

실험 절차

Using the method of Example 31, 3-amino-4-[2-(phenyl)ethylamino]quinoline was reacted with triethyl orthoformate and formic acid to provide 1-[2-(phenyl)ethyl]-1H-imidazo[4,5-c]quinoline, m.p. 105°-108° C.

출처 및 근거

ORD 기록
ord-88618bfd351a40df87e724b2284ff983
출처 데이터셋
uspto-grants-1987_08
특허 번호
US04689338

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