Ethylene carbonate → HCID 233168, 화합물

HRID 1789714노트

반응식

[CH2:1]1[O:5][C:4]2[CH:6]=[C:7]([OH:10])[CH:8]=[CH:9][C:3]=2[O:2]1.C1(=O)O[CH2:14][CH2:13][O:12]1>>[O:2]1[C:3]2[CH:9]=[CH:8][C:7]([O:10][CH2:14][CH2:13][OH:12])=[CH:6][C:4]=2[O:5][CH2:1]1

참가 물질

반응물 2

HCID 7303Ethylene carbonate

HCID 68289Sesamol

생성물 1

HCID 233168HCID 233168, 화합물수율 99%

실험 절차

The title compound was prepared according to the procedure of Example 114, Step 1 starting from sesamol (2.0 g, 14.5 mmol) and ethylene carbonate (1.0 g, 11.4 mmol): solid; yield 99%. MS m/z 182 (M)+.

출처 및 근거

ORD 기록: ord-e18f3809ac8644f1a2aa1e01f217bbeb
출처 데이터셋: uspto-grants-2006_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07071180B2

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